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Principles and practices of method validation
Title
Principles and practices of method validation / edited by A. Fajgelj, Á. Ambrus.
ISBN
9781847551757
1847551750
0854047832
9780854047833
Published
Cambridge : Royal Society of Chemistry, ©2000.
Physical Description
1 online resource (x, 305 pages) : illustrations
Local Notes
Each online book link provides access to a distinct volume of this title.
Access is available to the Yale community.
Notes
Proceedings of the Joint AOAC/FAO/IAEA/IUPAC International Workshop on the Principles and Practices of Method Validation held in November 1999 in Budapest, Hungary.
English.
Access and use
Access restricted by licensing agreement.
Summary
This product is not available separately, it is only sold as part of a set. There are 750 products in the set and these are all sold as one entity. Principles and Practices of Method Validation is an overview of the most recent approaches used for method validation in cases when a large number of analytes are determined from a single aliquot and where a large number of samples are to be analysed. Much of the content relates to the validation of new methods for pesticide residue analysis in foodstuffs and water but the principles can be applied to other similar fields of analysis. Different chromatographic methods are discussed, including estimation of various effects, eg. matrix-induced effects and the influence of the equipment set-up. The methods used for routine purposes and the validation of analytical data in the research and development environment are documented. The legislation covering the EU-Guidance on residue analytical methods, an extensive review of the existing in-house method validation documentation and guidelines for single-laboratory validation of analytical methods for trace-level concentrations of organic chemicals are also included. With contributions from experts in the field, any practising analyst dealing with method validation will find the examples presented in this book a useful source of technical information.
Variant and related titles
Royal society of chemistry 1968-2006. OCLC KB.
Other formats
Print version: Joint AOAC/FAO/IAEA/IUPAC International Workshop on the Principles and Practices of Method Validation (1999 : Budapest, Hungary). Principles and practices of method validation. Cambridge : Royal Society of Chemistry, ©2000
Format
Books / Online
Language
English
Added to Catalog
March 04, 2021
Series
Special publication ; no. 256
Bibliography
Includes bibliographical references and index.
Contents
The potential use of quality control data to validate pesticide residue method performance
Optimism and evaluation of multi-residue methods for priority pesticide in drinking and related waters
Validation of analytical data in a research and development environment
Performance validation of a multi-residue method for 170 pesticides in kiwifruit
Effects of sample processing on pesticide residues in fruit and vegetables
Testing efficiency and uncertainty of sample processing using 14C-labelled chlorpyrifos : part 1, Description of the methodology
Testing efficiency and uncertainty of sample processing using 14C-labelled chlorpyrifos, part 2
Testing the effect of sample processing and storage on the stability of residues
AOAC International collaborative study on the determination of pesticide residue in nonfatty foods by supercritical fluid extraction and gas chromatography/mass spectrometry
Validation of analytical methods-proving your methods is 'fit for purpose'
Validation of a multi-residue method for analysis of pesticides in fruit, vegetables and cereals by a GC/MS iontrap system
Development and validation of a generic gas chromatographic method for the determination of organophosphorous pesticide residues in various sample extracts
Validation of gas chromatographic databases for qualitative identification of active ingredients of pesticide residues
Estimation of significance of 'matrix-induced' chromatographic effects
Worked example of validation of a multi-residue method
EU guidance documents on redue analytical methods
Guidelines for single-laboratory validation of analytical methods for trace-level concentrations of organic chemicals
A critique on available in-house method validation documentation.
Subjects
Genre/Form
Electronic books.
Conference papers and proceedings.
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